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In Situ Spatial and Time-Resolved Studies of...
Journal article

In Situ Spatial and Time-Resolved Studies of Electrochemical Reactions by Scanning Transmission X-ray Microscopy

Abstract

The first in situ measurements with scanning transmission X-ray microscopy (STXM) of an active electrochemical cell are reported. An electrochemical wet cell, consisting of an electrodeposited polyaniline thin film on a thin Au film covered by an overlayer of 1 M HCl solution sitting between two X-ray transparent silicon nitride windows, was assembled. X-ray absorption images and spatial and time-resolved spectra of this system under potential …

Authors

Guay D; Stewart-Ornstein J; Zhang X; Hitchcock AP

Journal

Analytical Chemistry, Vol. 77, No. 11, pp. 3479–3487

Publisher

American Chemical Society (ACS)

Publication Date

June 1, 2005

DOI

10.1021/ac048077j

ISSN

0003-2700