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Analysis and Parametric Optimization of 1H...
Journal article

Analysis and Parametric Optimization of 1H Off-Resonance Relaxation NMR Experiments Designed to Map Polypeptide Self-Recognition and Other Noncovalent Interactions

Abstract

The measurement of 1H off-resonance nonselective relaxation rates (R(theta,ns)) has been recently proposed as an effective method to probe peptide self-recognition, opening new perspectives in the understanding of the prefibrillization oligomerization processes in amylodogenesis. However, a full analysis and parametric optimization of the NMR experiments designed to measure R(theta,ns) relaxation rates is still missing. Here we analyze the …

Authors

Milojevic J; Esposito V; Das R; Melacini G

Journal

The Journal of Physical Chemistry B, Vol. 110, No. 41, pp. 20664–20670

Publisher

American Chemical Society (ACS)

Publication Date

October 1, 2006

DOI

10.1021/jp063194z

ISSN

1520-6106