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Catalytic Oxidation of Binap on (Binap)Rh(Co)ci
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Catalytic Oxidation of Binap on (Binap)Rh(Co)ci

Abstract

The square planar complex, (BINAP)Rh(CO)Cl (BINAP 2,2’-bis(diphenylphosphino)-1,1’-binapthyl) was synthesised from [Rh(COD)Cl]2 (COD = 1,5 cyclooctadiene) and BINAP under a CO atmosphere. This complex reacts with oxygen to form the square-planar complex (BINAP(O))Rh(CO)Cl in approximately 50% yield, along with free BINAP dioxide (BINAP(O)2). The evolution of CO2 gas and the formation of other unidentified products were also detected. In the …

Authors

Bunten KA; Farrar DH; Lough A; Poë AJ

Pagination

pp. 375-381

Publisher

Springer Nature

Publication Date

2002

DOI

10.1007/978-94-010-0554-8_24

Conference proceedings

NATO Science Series II: Mathematics, Physics and Chemistry

ISSN

1568-2609

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