Journal article
Structural study of sulfamic acid at 4.2 K by ENDOR-detected NMR
Abstract
The electron–nuclear double resonance method (ENDOR) is used to obtain greatly enhanced NMR signals from the distant deuterium nuclei of perdeuterated sulfamic acid (ND3SO3) in single crystals at 4.2 K. The structural information is obtained by measuring the quadrupole coupling tensors of the deuterium atoms and their direction cosines. There is very good agreement between the N–D bond angles derived from these ENDOR-detected NMR (EDNMR) …
Authors
Reuveni A; Marcellus D; Parker RS; Kwiram AL
Journal
The Journal of Chemical Physics, Vol. 74, No. 1, pp. 179–183
Publisher
AIP Publishing
Publication Date
January 1, 1981
DOI
10.1063/1.440860
ISSN
0021-9606