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A portable high-field pulsed-magnet system for...
Journal article

A portable high-field pulsed-magnet system for single-crystal x-ray scattering studies

Abstract

We present a portable pulsed-magnet system for x-ray studies of materials in high magnetic fields (up to 30 T). The apparatus consists of a split-pair of minicoils cooled on a closed-cycle cryostat, which is used for x-ray diffraction studies with applied field normal to the scattering plane. A second independent closed-cycle cryostat is used for cooling the sample to near liquid helium temperatures. Pulsed magnetic fields (approximately 1 ms in total duration) are generated by discharging a configurable capacitor bank into the magnet coils. Time-resolved scattering data are collected using a combination of a fast single-photon counting detector, a multichannel scaler, and a high-resolution digital storage oscilloscope. The capabilities of this instrument are used to study a geometrically frustrated system revealing strong magnetostrictive effects in the spin-liquid state.

Authors

Islam Z; Ruff JPC; Nojiri H; Matsuda YH; Ross KA; Gaulin BD; Qu Z; Lang JC

Journal

Review of Scientific Instruments, Vol. 80, No. 11,

Publisher

AIP Publishing

Publication Date

November 1, 2009

DOI

10.1063/1.3251273

ISSN

0034-6748

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