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Microwave-assisted hydrothermal synthesis and...
Journal article

Microwave-assisted hydrothermal synthesis and electrochemical characterization of niobium pentoxide/carbon nanotubes composites

Abstract

This study reports the fabrication of high mass loading (32 mg/cm2) electrodes of niobium pentoxide (Nb2O5) nanoparticles and carbon nanotubes (CNTs) using a facile procedure. The as-obtained Nb2O5 nanoparticles by microwave-assisted hydrothermal synthesis presented pseudohexagonal (TT) phase, and when exposed to the thermal treatment, the Nb2O5 nanoparticles changed to orthorhombic (T) phase. Distinct morphologies were obtained, which …

Authors

Silva RM; Noremberg BS; Marins NH; Milne J; Zhitomirsky I; Carreño NLV

Journal

Journal of Materials Research, Vol. 34, No. 4, pp. 592–599

Publisher

Springer Nature

Publication Date

February 28, 2019

DOI

10.1557/jmr.2018.444

ISSN

0884-2914