Journal article
Problems, artifacts and solutions in the INADEQUATE NMR experiment
Abstract
The INADEQUATE experiment can provide unequalled, detailed information about the carbon skeleton of an organic molecule. However, it also has the reputation of requiring unreasonable amounts of sample. Modern spectrometers and probes have mitigated this problem, and it is now possible to get good structural data on a few milligrams of a typical organic small molecule. In this paper, we analyze the experiment step by step in some detail, to show …
Authors
Bain AD; Hughes DW; Anand CK; Nie Z; Robertson VJ
Journal
Magnetic Resonance in Chemistry, Vol. 48, No. 8, pp. 630–641
Publisher
Wiley
Publication Date
August 2010
DOI
10.1002/mrc.2639
ISSN
0749-1581