Ultra-stable Co3O4/NiCo2O4 double-shelled hollow nanocages as headspace solid-phase microextraction coating for enhanced capture of polychlorinated biphenyls

Polychlorinated biphenyls (PCBs) are persistent toxic pollutants that tend to accumulate in food and cause damage to human health. This work reports the ultra-sensitive detection of PCBs in beverage samples (green tea, honey, and bottled drinking water) by headspace solid-phase microextraction (HS-SPME) coupled with a gas chromatography-flame ionization detector (GC-FID). The Ultra-stable Co3O4/NiCo2O4 double-shelled hollow nanocages (DSHNC) as …