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The preparation and characterization of iron...
Journal article

The preparation and characterization of iron trihydroxide, Fe(OH)3

Abstract

Iron trihydroxide has been prepared by the oxidation of FeSO 4 with [Co(III)(en)(dien)] 2 O 2 [ClO 4 ] 4 , [Co(III)(tetraen)] 2 O 2 [ClO 4 ] 4 , and H 2 O 2 in acid solution. These materials have been characterized by DTA, magnetic susceptibility, Mössbauer spectroscopy. X-ray powder diffraction, and electron microscopy. Particle sizes are found to be ~80 Å in diameter, but in the case of the (tetraen) preparation we find needle-like …

Authors

Au-Yeung SCF; Eaton DR; Birchall T; Dns G; Greedan JE; Hallett C; Ruebenbauer K

Journal

Canadian Journal of Chemistry, Vol. 63, No. 12, pp. 3378–3385

Publisher

Canadian Science Publishing

Publication Date

December 1, 1985

DOI

10.1139/v85-557

ISSN

0008-4042

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