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Four-Dimensional Imaging of ZnO-Coated Alumina...
Journal article

Four-Dimensional Imaging of ZnO-Coated Alumina Aerogels by Scanning Transmission X‑ray Microscopy and Ptychographic Tomography

Abstract

Functional porous materials are of increasing importance in energy conversion and catalysis. Improved analysis is needed to guide optimization. Four-dimensional (4D) imaging [chemical mapping in three-dimensional (3D) by spectro-tomography] of an Al2O3 aerogel coated with ZnO by atomic layer deposition was performed using soft X-ray ptychography at the Zn L-edge. A two-dimensional spatial resolution of 14(2) nm was achieved. Visualizations of …

Authors

Wu J; Zhu X; Shapiro DA; Lee JRI; Van Buuren T; Biener MM; Gammon SA; Li TT; Baumann TF; Hitchcock AP

Journal

The Journal of Physical Chemistry C, Vol. 122, No. 44, pp. 25374–25385

Publisher

American Chemical Society (ACS)

Publication Date

November 8, 2018

DOI

10.1021/acs.jpcc.8b07363

ISSN

1932-7447