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Integrated Solid-Phase Synthesis and Purification...
Journal article

Integrated Solid-Phase Synthesis and Purification of PEGylated Protein

Abstract

We describe an integrated method for solid-phase protein PEGylation and the purification of mono-PEGylated protein thus synthesized. Lysozyme was used as model protein in this study. Methoxy-polyethyleneglycol propionaldehyde (or m-PEG propionaldehyde) was first immobilized on a stack of microporous hydrophobic interaction membranes housed in a module. The membrane-bound m-PEG propionaldehyde was then contacted with lysozyme solution, which …

Authors

Shang X; Yu D; Ghosh R

Journal

Biomacromolecules, Vol. 12, No. 7, pp. 2772–2779

Publisher

American Chemical Society (ACS)

Publication Date

July 11, 2011

DOI

10.1021/bm200541r

ISSN

1525-7797