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In Situ Studies of Copper-Based CO2 Reduction...
Journal article

In Situ Studies of Copper-Based CO2 Reduction Electrocatalysts by Scanning Transmission Soft X‑ray Microscopy

Abstract

A microfluidic-enabled electrochemical device has been developed to investigate electrochemically active nanomaterials under reaction conditions using in situ scanning transmission soft X-ray microscopy (STXM). In situ STXM measurements were conducted on electrodeposited Cu catalysts under electrochemical CO2 reduction (CO2R) conditions. The study provides detailed, quantitative results about the changes in the morphology and chemical structure …

Authors

Zhang C; Eraky H; Tan S; Hitchcock A; Higgins D

Journal

ACS Nano, Vol. 17, No. 21, pp. 21337–21348

Publisher

American Chemical Society (ACS)

Publication Date

November 14, 2023

DOI

10.1021/acsnano.3c05964

ISSN

1936-0851