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Size-Selected Synthesis of PtRu Nano-Catalysts:...
Journal article

Size-Selected Synthesis of PtRu Nano-Catalysts: Reaction and Size Control Mechanism

Abstract

A rapid synthesis method for the preparation of PtRu colloids and their subsequent deposition on high surface area carbons is presented. The reaction mechanism is shown to involve the oxidation of the solvent, ethylene glycol, to mainly glycolic acid or, depending on the pH, its anion, glycolate, while the Pt(+IV) and Ru(+III) precursor salts are reduced. Glycolate acts as a stabilizer for the PtRu colloids and the glycolate concentration, and …

Authors

Bock C; Paquet C; Couillard M; Botton GA; MacDougall BR

Journal

Journal of the American Chemical Society, Vol. 126, No. 25, pp. 8028–8037

Publisher

American Chemical Society (ACS)

Publication Date

June 1, 2004

DOI

10.1021/ja0495819

ISSN

0002-7863