Journal article
Instrumentation for in situ flow electrochemical Scanning Transmission X-ray Microscopy (STXM)
Abstract
We report the design and performance of a 3-electrode device for real time in situ scanning transmission X-ray microscopy studies of electrochemical processes under both static (sealed, non-flow) conditions and with a continuous flow of electrolytes. The device was made using a combination of silicon microfabrication and 3D printing technologies. The performance is illustrated by results of a study of copper deposition and stripping at a gold …
Authors
Prabu V; Obst M; Hosseinkhannazer H; Reynolds M; Rosendahl S; Wang J; Hitchcock AP
Journal
Review of Scientific Instruments, Vol. 89, No. 6,
Publisher
AIP Publishing
Publication Date
June 1, 2018
DOI
10.1063/1.5023288
ISSN
0034-6748