A Universal Roadmap for Quantification of Glycerol Electrooxidation Products Using Proton Nuclear Magnetic Spectroscopy (1H NMR)

The electrochemical oxidation of glycerol, a byproduct of biofuel production, can transform this low-value material into a range of valuable compounds to foster a circular bioeconomy. However, developing catalysts and unraveling the mechanisms behind glycerol oxidation hinge on the precise quantification of reaction products, a task requiring analytical techniques. Our research introduces proton nuclear magnetic spectroscopy (1H NMR) as a …