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Alkynylcyclohexanol Chairs and Twist-Boats:...
Journal article

Alkynylcyclohexanol Chairs and Twist-Boats: Co2(CO)6 as a Conformational Switch

Abstract

Treatment of 1-[axial]-(trimethylsilylethynyl)cyclohexan-1-ol with dicobalt octacarbonyl results in a conformational ring flip such that the bulky dicobalt-alkyne cluster moiety now occupies the favored equatorial site. However, when a 4-tert-butyl substituent is present, the coordinated alkynyl group retains its original axial or equatorial position. Complexation of trans-[diaxial]-1,4-bis(triphenylsilylethynyl)cyclohexane-1,4-diol brings …

Authors

Deschamps NM; Kaldis JH; Lock PE; Britten JF; McGlinchey MJ

Journal

The Journal of Organic Chemistry, Vol. 66, No. 25, pp. 8585–8591

Publisher

American Chemical Society (ACS)

Publication Date

December 1, 2001

DOI

10.1021/jo0108820

ISSN

0022-3263