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Generation and characterization of ionic and...
Journal article

Generation and characterization of ionic and neutral (CH3OBH)+/· and (CH3BOH)+/· in the gas phase by tandem mass spectrometry

Abstract

The isomeric dicoordinated borinium ions CH3O–B–H+ and CH3–B–OH+ are generated upon electron ionization of trimethylborate and methyl boronic acid, respectively. The connectivity of the ions is confirmed by collision-induced dissociation experiments on magnetic deflection type tandem mass spectrometers. Neutralization–reionization experiments on these structurally characterized ions indicate that the neutral radicals CH3O–B–H· and CH3–B–OH· are …

Authors

Srinivas R; Vivekananda S; Blanksby SJ; Schröder D; Trikoupis MA; Terlouw JK; Schwarz H

Journal

International Journal of Mass Spectrometry, Vol. 202, No. 1-3, pp. 315–322

Publisher

Elsevier

Publication Date

October 2000

DOI

10.1016/s1387-3806(00)00256-6

ISSN

1387-3806